Nov 29, 2018

Gumos akceleratoriaus CBS paruošimo metodas

Palik žinutę

Šis išradimas yra paruošiamas   guma   ypač cheminių medžiagų, yra susijęs su a   guma   akceleratorius   CBS .


China's   rubber   industry in recent years has achieved sustained, rapid and healthy development. China's   rubber   industry in recent years has achieved sustained, rapid and healthy development. China's   rubber   industry in recent years has achieved sustained, rapid and healthy development.   Raw   rubber   consumption for six consecutive years to maintain the world, are growing at double-digit rates each year. Raw   rubber   consumption for six consecutive years to maintain the world, are growing at double-digit rates each year. Raw   rubber   consumption for six consecutive years to maintain the world, are growing at double-digit rates each year.   It provides a broad market space for the development of   rubber   chemicals. It provides a broad market space for the development of   rubber   chemicals. It provides a broad market space for the development of   rubber   chemicals.   2001-- 2007   rubber   accelerator   average annual growth rate of 28%. 2001-- 2007   rubber   accelerator   average annual growth rate of 28%. 2001-- 2007   rubber   accelerator   average annual growth rate of 28%. 2001-- 2007   rubber   accelerator   average annual growth rate of 28%. 2001-- 2007   rubber   accelerator   average annual growth rate of 28%.   Wherein   Accelerator   CBS   annual growth rate of 36X. Wherein   Accelerator   CBS   annual growth rate of 36X. Wherein   Accelerator   CBS   annual growth rate of 36X. Wherein   Accelerator   CBS   annual growth rate of 36X. Wherein   Accelerator   CBS   annual growth rate of 36X.


Accelerator   CBS   chemical name is N--cyclohexyl-2 - benzothiazole sulfenamide, green adjuvants, is one of the common delayed action accelerators, both short scorch resistance and excellent cure time of two advantages, and other promoters may also increase when a predetermined vulcanized   rubber   tensile strength and elongation. Accelerator   CBS   chemical name is N--cyclohexyl-2 - benzothiazole sulfenamide, green adjuvants, is one of the common delayed action accelerators, both short scorch resistance and excellent cure time of two advantages, and other promoters may also increase when a predetermined vulcanized   rubber   tensile strength and elongation. Accelerator   CBS   chemical name is N--cyclohexyl-2 - benzothiazole sulfenamide, green adjuvants, is one of the common delayed action accelerators, both short scorch resistance and excellent cure time of two advantages, and other promoters may also increase when a predetermined vulcanized   rubber   tensile strength and elongation. Accelerator   CBS   chemical name is N--cyclohexyl-2 - benzothiazole sulfenamide, green adjuvants, is one of the common delayed action accelerators, both short scorch resistance and excellent cure time of two advantages, and other promoters may also increase when a predetermined vulcanized   rubber   tensile strength and elongation. Accelerator   CBS   chemical name is N--cyclohexyl-2 - benzothiazole sulfenamide, green adjuvants, is one of the common delayed action accelerators, both short scorch resistance and excellent cure time of two advantages, and other promoters may also increase when a predetermined vulcanized   rubber   tensile strength and elongation. Accelerator   CBS   chemical name is N--cyclohexyl-2 - benzothiazole sulfenamide, green adjuvants, is one of the common delayed action accelerators, both short scorch resistance and excellent cure time of two advantages, and other promoters may also increase when a predetermined vulcanized   rubber   tensile strength and elongation.   Slight color change, no blooming, good vulcanizate aging properties. Particularly suitable for the production of radial tires.


1, A method of preparing   rubber   accelerator   CBS   agent, characterized in that: comprising the steps of: (1) Synthesis of M crude   rubber accelerator ; (2) prepared using a crude M   CBS . A method of preparing   rubber   accelerator   CBS   agent, characterized in that: comprising the steps of: (1) Synthesis of M crude   rubber accelerator ; (2) prepared using a crude M   CBS . A method of preparing   rubber   accelerator   CBS   agent, characterized in that: comprising the steps of: (1) Synthesis of M crude   rubber accelerator ; (2) prepared using a crude M   CBS . A method of preparing   rubber   accelerator   CBS   agent, characterized in that: comprising the steps of: (1) Synthesis of M crude   rubber accelerator ; (2) prepared using a crude M   CBS . A method of preparing   rubber   accelerator   CBS   agent, characterized in that: comprising the steps of: (1) Synthesis of M crude   rubber accelerator ; (2) prepared using a crude M   CBS . A method of preparing   rubber   accelerator   CBS   agent, characterized in that: comprising the steps of: (1) Synthesis of M crude   rubber accelerator ; (2) prepared using a crude M   CBS . A method of preparing   rubber   accelerator   CBS   agent, characterized in that: comprising the steps of: (1) Synthesis of M crude   rubber accelerator ; (2) prepared using a crude M   CBS . A method of preparing   rubber   accelerator   CBS   agent, characterized in that: comprising the steps of: (1) Synthesis of M crude   rubber accelerator ; (2) prepared using a crude M   CBS . A method of preparing   rubber   accelerator   CBS   agent, characterized in that: comprising the steps of: (1) Synthesis of M crude   rubber accelerator ; (2) prepared using a crude M   CBS . A method of preparing   rubber   accelerator   CBS   agent, characterized in that: comprising the steps of: (1) Synthesis of M crude   rubber accelerator ; (2) prepared using a crude M   CBS . A method of preparing   rubber   accelerator   CBS   agent, characterized in that: comprising the steps of: (1) Synthesis of M crude   rubber accelerator ; (2) prepared using a crude M   CBS . A method of preparing   rubber   accelerator   CBS   agent, characterized in that: comprising the steps of: (1) Synthesis of M crude   rubber accelerator ; (2) prepared using a crude M   CBS . A method of preparing   rubber   accelerator   CBS   agent, characterized in that: comprising the steps of: (1) Synthesis of M crude   rubber accelerator ; (2) prepared using a crude M   CBS .


2, The method of preparing   rubber   accelerator   CBS   claimed in claim 1, characterized in that - the step (1), the carbon disulfide, sulfur, sulfur formulated solution was gravity of 1.3-1.5, parts by weight of the aniline and 350-450 500-600 parts by weight of sulfur dissolved pumped into the autoclave, the autoclave temperature 260 -300 ° C, a pressure 8-10Mpa, reacted for 5 - 8 hours the crude synthetic   rubber   accelerator   M. 2, The method of preparing   rubber   accelerator   CBS   claimed in claim 1, characterized in that - the step (1), the carbon disulfide, sulfur, sulfur formulated solution was gravity of 1.3-1.5, parts by weight of the aniline and 350-450 500-600 parts by weight of sulfur dissolved pumped into the autoclave, the autoclave temperature 260 -300 ° C, a pressure 8-10Mpa, reacted for 5 - 8 hours the crude synthetic   rubber   accelerator   M. 2, The method of preparing   rubber   accelerator   CBS   claimed in claim 1, characterized in that - the step (1), the carbon disulfide, sulfur, sulfur formulated solution was gravity of 1.3-1.5, parts by weight of the aniline and 350-450 500-600 parts by weight of sulfur dissolved pumped into the autoclave, the autoclave temperature 260 -300 ° C, a pressure 8-10Mpa, reacted for 5 - 8 hours the crude synthetic   rubber   accelerator   M. 2, The method of preparing   rubber   accelerator   CBS   claimed in claim 1, characterized in that - the step (1), the carbon disulfide, sulfur, sulfur formulated solution was gravity of 1.3-1.5, parts by weight of the aniline and 350-450 500-600 parts by weight of sulfur dissolved pumped into the autoclave, the autoclave temperature 260 -300 ° C, a pressure 8-10Mpa, reacted for 5 - 8 hours the crude synthetic   rubber   accelerator   M. 2, The method of preparing   rubber   accelerator   CBS   claimed in claim 1, characterized in that - the step (1), the carbon disulfide, sulfur, sulfur formulated solution was gravity of 1.3-1.5, parts by weight of the aniline and 350-450 500-600 parts by weight of sulfur dissolved pumped into the autoclave, the autoclave temperature 260 -300 ° C, a pressure 8-10Mpa, reacted for 5 - 8 hours the crude synthetic   rubber   accelerator   M. 2, The method of preparing   rubber   accelerator   CBS   claimed in claim 1, characterized in that - the step (1), the carbon disulfide, sulfur, sulfur formulated solution was gravity of 1.3-1.5, parts by weight of the aniline and 350-450 500-600 parts by weight of sulfur dissolved pumped into the autoclave, the autoclave temperature 260 -300 ° C, a pressure 8-10Mpa, reacted for 5 - 8 hours the crude synthetic   rubber   accelerator   M. 2, The method of preparing   rubber   accelerator   CBS   claimed in claim 1, characterized in that - the step (1), the carbon disulfide, sulfur, sulfur formulated solution was gravity of 1.3-1.5, parts by weight of the aniline and 350-450 500-600 parts by weight of sulfur dissolved pumped into the autoclave, the autoclave temperature 260 -300 ° C, a pressure 8-10Mpa, reacted for 5 - 8 hours the crude synthetic   rubber   accelerator   M. 2, The method of preparing   rubber   accelerator   CBS   claimed in claim 1, characterized in that - the step (1), the carbon disulfide, sulfur, sulfur formulated solution was gravity of 1.3-1.5, parts by weight of the aniline and 350-450 500-600 parts by weight of sulfur dissolved pumped into the autoclave, the autoclave temperature 260 -300 ° C, a pressure 8-10Mpa, reacted for 5 - 8 hours the crude synthetic   rubber   accelerator   M. 2, The method of preparing   rubber   accelerator   CBS   claimed in claim 1, characterized in that - the step (1), the carbon disulfide, sulfur, sulfur formulated solution was gravity of 1.3-1.5, parts by weight of the aniline and 350-450 500-600 parts by weight of sulfur dissolved pumped into the autoclave, the autoclave temperature 260 -300 ° C, a pressure 8-10Mpa, reacted for 5 - 8 hours the crude synthetic   rubber   accelerator   M. 2, The method of preparing   rubber   accelerator   CBS   claimed in claim 1, characterized in that - the step (1), the carbon disulfide, sulfur, sulfur formulated solution was gravity of 1.3-1.5, parts by weight of the aniline and 350-450 500-600 parts by weight of sulfur dissolved pumped into the autoclave, the autoclave temperature 260 -300 ° C, a pressure 8-10Mpa, reacted for 5 - 8 hours the crude synthetic   rubber   accelerator   M. 2, The method of preparing   rubber   accelerator   CBS   claimed in claim 1, characterized in that - the step (1), the carbon disulfide, sulfur, sulfur formulated solution was gravity of 1.3-1.5, parts by weight of the aniline and 350-450 500-600 parts by weight of sulfur dissolved pumped into the autoclave, the autoclave temperature 260 -300 ° C, a pressure 8-10Mpa, reacted for 5 - 8 hours the crude synthetic   rubber   accelerator   M.


3, The method of preparing   rubber   accelerator   CBS   claimed in claim 2, wherein: the step (2) consists of the following steps in sequence of: a oxide: 1000-2000 cyclohexylamine parts by weight of 30 wt dubbed -50% aqueous solution, an aqueous solution of cyclohexylamine as a solvent, the obtained crude product M completely dissolved, dissolution temperature 60_ 100 ° C, _2 dissolution time of 1 hour, the dissolving liquid into the oxidation reactor, in parts by weight of 1650-2750 sodium hypochlorite as the oxidant, the oxidation temperature 20 - 5 (TC, oxidation time of 3 - 6 hours;. B washing, dewatering, drying, packaging products. 3, The method of preparing   rubber   accelerator   CBS   claimed in claim 2, wherein: the step (2) consists of the following steps in sequence of: a oxide: 1000-2000 cyclohexylamine parts by weight of 30 wt dubbed -50% aqueous solution, an aqueous solution of cyclohexylamine as a solvent, the obtained crude product M completely dissolved, dissolution temperature 60_ 100 ° C, _2 dissolution time of 1 hour, the dissolving liquid into the oxidation reactor, in parts by weight of 1650-2750 sodium hypochlorite as the oxidant, the oxidation temperature 20 - 5 (TC, oxidation time of 3 - 6 hours;. B washing, dewatering, drying, packaging products. 3, The method of preparing   rubber   accelerator   CBS   claimed in claim 2, wherein: the step (2) consists of the following steps in sequence of: a oxide: 1000-2000 cyclohexylamine parts by weight of 30 wt dubbed -50% aqueous solution, an aqueous solution of cyclohexylamine as a solvent, the obtained crude product M completely dissolved, dissolution temperature 60_ 100 ° C, _2 dissolution time of 1 hour, the dissolving liquid into the oxidation reactor, in parts by weight of 1650-2750 sodium hypochlorite as the oxidant, the oxidation temperature 20 - 5 (TC, oxidation time of 3 - 6 hours;. B washing, dewatering, drying, packaging products. 3, The method of preparing   rubber   accelerator   CBS   claimed in claim 2, wherein: the step (2) consists of the following steps in sequence of: a oxide: 1000-2000 cyclohexylamine parts by weight of 30 wt dubbed -50% aqueous solution, an aqueous solution of cyclohexylamine as a solvent, the obtained crude product M completely dissolved, dissolution temperature 60_ 100 ° C, _2 dissolution time of 1 hour, the dissolving liquid into the oxidation reactor, in parts by weight of 1650-2750 sodium hypochlorite as the oxidant, the oxidation temperature 20 - 5 (TC, oxidation time of 3 - 6 hours;. B washing, dewatering, drying, packaging products. 3, The method of preparing   rubber   accelerator   CBS   claimed in claim 2, wherein: the step (2) consists of the following steps in sequence of: a oxide: 1000-2000 cyclohexylamine parts by weight of 30 wt dubbed -50% aqueous solution, an aqueous solution of cyclohexylamine as a solvent, the obtained crude product M completely dissolved, dissolution temperature 60_ 100 ° C, _2 dissolution time of 1 hour, the dissolving liquid into the oxidation reactor, in parts by weight of 1650-2750 sodium hypochlorite as the oxidant, the oxidation temperature 20 - 5 (TC, oxidation time of 3 - 6 hours;. B washing, dewatering, drying, packaging products. 3, The method of preparing   rubber   accelerator   CBS   claimed in claim 2, wherein: the step (2) consists of the following steps in sequence of: a oxide: 1000-2000 cyclohexylamine parts by weight of 30 wt dubbed -50% aqueous solution, an aqueous solution of cyclohexylamine as a solvent, the obtained crude product M completely dissolved, dissolution temperature 60_ 100 ° C, _2 dissolution time of 1 hour, the dissolving liquid into the oxidation reactor, in parts by weight of 1650-2750 sodium hypochlorite as the oxidant, the oxidation temperature 20 - 5 (TC, oxidation time of 3 - 6 hours;. B washing, dewatering, drying, packaging products. 3, The method of preparing   rubber   accelerator   CBS   claimed in claim 2, wherein: the step (2) consists of the following steps in sequence of: a oxide: 1000-2000 cyclohexylamine parts by weight of 30 wt dubbed -50% aqueous solution, an aqueous solution of cyclohexylamine as a solvent, the obtained crude product M completely dissolved, dissolution temperature 60_ 100 ° C, _2 dissolution time of 1 hour, the dissolving liquid into the oxidation reactor, in parts by weight of 1650-2750 sodium hypochlorite as the oxidant, the oxidation temperature 20 - 5 (TC, oxidation time of 3 - 6 hours;. B washing, dewatering, drying, packaging products.


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